PY3010 PILOT PLANT AND SCALE UP METHODS SYLLABUS | ANNA UNIVERSITY BTECH PHARMACEUTICAL 8TH SEMESTER SYLLABUS REGULATION 2008 2011 2012-2013 BELOW IS THE ANNA UNIVERSITY 8TH SEMESTER B.TECH PHARMACEUTICAL DEPARTMENT SYLLABUS, TEXTBOOKS, REFERENCE BOOKS,EXAM PORTIONS,QUESTION BANK,PREVIOUS YEAR QUESTION PAPERS,MODEL QUESTION PAPERS, CLASS NOTES, IMPORTANT 2 MARKS, 8 MARKS, 16 MARKS TOPICS. IT IS APPLICABLE FOR ALL STUDENTS ADMITTED IN THE YEAR 2011 2012-2013 (ANNA UNIVERSITY CHENNAI,TRICHY,MADURAI, TIRUNELVELI,COIMBATORE), 2008 REGULATION OF ANNA UNIVERSITY CHENNAI AND STUDENTS ADMITTED IN ANNA UNIVERSITY CHENNAI DURING 2009
PY3010 PILOT PLANT AND SCALE UP METHODS
UNIT I NECESSITY AND PURPOSE 9
Function – Size estimation – Location personnel requirements – Operation programming
– Sampling data – Report of results – Cost factor – Safety factors.
UNIT II PRINCIPLE 9
Principle of similarity – Dimensional analysis – Scale up equations – Extrapolations –
Analog models.
L T P C
3 0 0 3
76
UNIT- III DESIGN 9
Pilot plant design for flow ducts – Mixing equipments – Heat transfer equipments.
UNIT- IV METHODS 9
Design methods for packed towers – Batch and continuous distillation columns.
UNIT- V EQUIPMENTS 9
Pilot plants for reactors – Furnaces – Filters and mechanical operations equipments.
TOTAL: 45 PERIODS
TEXT BOOKS
1. Bisio, A. and Kabel, R.L., “Scale Up of Chemical Processes”, John Wiley
Publishers, 1990.
2. Johnstone, R.E. and Thring, M.W., “Pilot Plants Models and Scale Up Methods in
Chemical Engineering”, McGraw Hill Book Co., 1987.
REFERENCES
1. Ernest, J. and Staffin, K.H., “Stage-wise Process Design”, John Wiley
Publications, 1989.
2. Levin, M., “Pharmaceutical Process Scale-Up”, Informa Healthcare, 2002.
3. Hynes, M.D., “Preparing for FDA Pre-approval Inspections”, Informa Healthcare,
1998.
PY3010 PILOT PLANT AND SCALE UP METHODS
UNIT I NECESSITY AND PURPOSE 9
Function – Size estimation – Location personnel requirements – Operation programming
– Sampling data – Report of results – Cost factor – Safety factors.
UNIT II PRINCIPLE 9
Principle of similarity – Dimensional analysis – Scale up equations – Extrapolations –
Analog models.
L T P C
3 0 0 3
76
UNIT- III DESIGN 9
Pilot plant design for flow ducts – Mixing equipments – Heat transfer equipments.
UNIT- IV METHODS 9
Design methods for packed towers – Batch and continuous distillation columns.
UNIT- V EQUIPMENTS 9
Pilot plants for reactors – Furnaces – Filters and mechanical operations equipments.
TOTAL: 45 PERIODS
TEXT BOOKS
1. Bisio, A. and Kabel, R.L., “Scale Up of Chemical Processes”, John Wiley
Publishers, 1990.
2. Johnstone, R.E. and Thring, M.W., “Pilot Plants Models and Scale Up Methods in
Chemical Engineering”, McGraw Hill Book Co., 1987.
REFERENCES
1. Ernest, J. and Staffin, K.H., “Stage-wise Process Design”, John Wiley
Publications, 1989.
2. Levin, M., “Pharmaceutical Process Scale-Up”, Informa Healthcare, 2002.
3. Hynes, M.D., “Preparing for FDA Pre-approval Inspections”, Informa Healthcare,
1998.
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