PC3010 MULTICOMPONENT DISTILLATION SYLLABUS | ANNA UNIVERSITY BE PETROCHEMICAL ENGINEERING 8TH SEMESTER SYLLABUS REGULATION 2008 2011 2012-2013 BELOW IS THE ANNA UNIVERSITY 8TH SEMESTER B.E PETROCHEMICAL ENGINEERING DEPARTMENT SYLLABUS, TEXTBOOKS, REFERENCE BOOKS,EXAM PORTIONS,QUESTION BANK,PREVIOUS YEAR QUESTION PAPERS,MODEL QUESTION PAPERS, CLASS NOTES, IMPORTANT 2 MARKS, 8 MARKS, 16 MARKS TOPICS. IT IS APPLICABLE FOR ALL STUDENTS ADMITTED IN THE YEAR 2011 2012-2013 (ANNA UNIVERSITY CHENNAI,TRICHY,MADURAI, TIRUNELVELI,COIMBATORE), 2008 REGULATION OF ANNA UNIVERSITY CHENNAI AND STUDENTS ADMITTED IN ANNA UNIVERSITY CHENNAI DURING 2009
PC3010 MULTICOMPONENT DISTILLATION L T P C
3 0 0 3
UNIT I THERMODYNAMIC PRINCIPLES 9
General considerations in the design of columns – Column sequencing – Heuristics for column
sequencing – Key components – Distributed components – Non-Distributed components –
Adjacent keys.
Fundamental Thermodynamic principles involved in the calculation of vapor – liquid equilibria and
enthalpies of multi component mixtures – Use of multiple equation of state for the calculation of K
values – Estimation of the fugacity coefficients for the vapor phase of polar gas mixtures –
calculation of liquid – phase activity coefficients.
UNIT II THERMODYNAMIC PROPERTY EVALUATION 9
Fundamental principles involved in the separation of multi component mixtures – Determination of
bubble-point and Dew Point Temperatures for multi component mixtures – equilibrium flash
distillation calculations for multi component mixtures – separation of multi component mixtures at
total reflux.
UNIT III MINIMUM REFLUX RATIO FOR MCD SYSTEM 9
Definition of minimum reflux ratio – calculation of Rm for multi component distillation – Underwood
method – Colburn method.
72
UNIT IV VARIOUS METHODS OF MCD COLUMN DESIGN 9
Theta method of convergence – Kb method and the constant composition method – Application of
the Theta method to complex columns and to system of columns – Lewis Matheson method –
Stage and reflux requirements – Short cut methods and Simplified graphical procedures.
U N I T V V AR IO US T Y P E S O F MC D CO L UMNS 9
Design of sieve, bubble cap, valve trays and structured packing columns for multi component
distillation – computation of plate efficiencies.
TOTAL: 60 PERIODS
TEXT BOOKS
1. Holland, C.D., “Fundamentals of Multi Component Distillation”, McGraw Hill Book Company,1981
2. Van Winkle, “Distillation Operations”, McGraw Hill Publications, 1987.
REFERENCES
1. King, C.J., “Separation Process Principles”, Mc Graw Publications, 1986.
2. Treybal, R.E., “Mass Ttransfer Operations”, 5th Edition, Mc Graw Hill publications. 1996.
3. Mc Cabe and Smith, J.C., Harriot, “Unit Operation of Chemical Engineering”, 6th Edition,
McGraw Hill, 2001.
PC3010 MULTICOMPONENT DISTILLATION L T P C
3 0 0 3
UNIT I THERMODYNAMIC PRINCIPLES 9
General considerations in the design of columns – Column sequencing – Heuristics for column
sequencing – Key components – Distributed components – Non-Distributed components –
Adjacent keys.
Fundamental Thermodynamic principles involved in the calculation of vapor – liquid equilibria and
enthalpies of multi component mixtures – Use of multiple equation of state for the calculation of K
values – Estimation of the fugacity coefficients for the vapor phase of polar gas mixtures –
calculation of liquid – phase activity coefficients.
UNIT II THERMODYNAMIC PROPERTY EVALUATION 9
Fundamental principles involved in the separation of multi component mixtures – Determination of
bubble-point and Dew Point Temperatures for multi component mixtures – equilibrium flash
distillation calculations for multi component mixtures – separation of multi component mixtures at
total reflux.
UNIT III MINIMUM REFLUX RATIO FOR MCD SYSTEM 9
Definition of minimum reflux ratio – calculation of Rm for multi component distillation – Underwood
method – Colburn method.
72
UNIT IV VARIOUS METHODS OF MCD COLUMN DESIGN 9
Theta method of convergence – Kb method and the constant composition method – Application of
the Theta method to complex columns and to system of columns – Lewis Matheson method –
Stage and reflux requirements – Short cut methods and Simplified graphical procedures.
U N I T V V AR IO US T Y P E S O F MC D CO L UMNS 9
Design of sieve, bubble cap, valve trays and structured packing columns for multi component
distillation – computation of plate efficiencies.
TOTAL: 60 PERIODS
TEXT BOOKS
1. Holland, C.D., “Fundamentals of Multi Component Distillation”, McGraw Hill Book Company,1981
2. Van Winkle, “Distillation Operations”, McGraw Hill Publications, 1987.
REFERENCES
1. King, C.J., “Separation Process Principles”, Mc Graw Publications, 1986.
2. Treybal, R.E., “Mass Ttransfer Operations”, 5th Edition, Mc Graw Hill publications. 1996.
3. Mc Cabe and Smith, J.C., Harriot, “Unit Operation of Chemical Engineering”, 6th Edition,
McGraw Hill, 2001.
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