PY3311 INSTRUMENTAL METHODS OF PHARMACEUTICAL ANALYSIS SYLLABUS | ANNA UNIVERSITY BTECH PHARMACEUTICAL TECHNOLOGY 6TH SEMESTER SYLLABUS REGULATION 2008 2011 2012-2013 BELOW IS THE ANNA UNIVERSITY SIXTH SEMESTER B.TECH PHARMACEUTICAL TECHNOLOGY DEPARTMENT SYLLABUS, TEXTBOOKS, REFERENCE BOOKS,EXAM PORTIONS,QUESTION BANK,PREVIOUS YEAR QUESTION PAPERS,MODEL QUESTION PAPERS, CLASS NOTES, IMPORTANT 2 MARKS, 8 MARKS, 16 MARKS TOPICS. IT IS APPLICABLE FOR ALL STUDENTS ADMITTED IN THE YEAR 2011 2012-2013 (ANNA UNIVERSITY CHENNAI,TRICHY,MADURAI, TIRUNELVELI,COIMBATORE), 2008 REGULATION OF ANNA UNIVERSITY CHENNAI AND STUDENTS ADMITTED IN ANNA UNIVERSITY CHENNAI DURING 2009
PY3311 INSTRUMENTAL METHODS OF PHARMACEUTICAL ANALYSIS
UNIT I UV – VISIBLE SPECTROSCOPY 9
Properties of electromagnetic spectrum – Chromophore concept – Beer’s and
Lambart’s law – Limitations – Theory of electronic spectroscopy – Choice of solvent and
solvent effects – Modern instrumentation – Design and working principle – Applications
of UV-Visible spectroscopy – Nephlometry and turbidimetry – Principle – Instrumentation
– Applications.
UNIT II INFRARED AND NMR SPECTROSCOPY 9
Principles of vibrational spectroscopy – Instrumentation and sampling techniques –
Applications in pharmaceutical sciences – NMR principles – Instrumentation –
Applications.
L T P C
0 0 3 2
L T P C
3 1 0 4
48
UNIT III MASS AND ATOMIC SPECTROSCOPY 9
Principles – Instrumentation – Ionization techniques – Electron impact ionization –
Chemical ionization – Applications – Atomic absorption spectroscopy – Principle –
Instrumentation – Applications.
UNIT IV CHROMATOGRAPHIC TECHNIQUES 9
Chromatographic methods – Paper chromatography – Thin layer chromatography – Ion
exchange chromatography – Column chromatography – High performance liquid
chromatography – Applications.
UNIT V ELCTROCHEMICAL METHODS OF ANALYSIS 9
Potentiometry – Types of electrodes – Measurement of EMF and pH – Applications –
Conductometry – Measurement of conductivity – Conductometric titrations.
L: 45 T: 15 TOTAL: 60 PERIODS
TEXT BOOKS
1. Beckett, A.K. and Stenlake, J.B., “Practical Pharmaceutical Chemistry”, Part I
and II, 4th Edition, CBS Publications, 1997.
2. Chatwal, G.R. and Anand, S.K., “Instrumental Methods of Chemical Analysis”,
Himalaya Publishing House, 2005.
REFERENCES
1. Willard, H.H., Merritt Jr, L.L., Dean, J.A. and Settle Jr, F.A., “Instrumental
Methods of Analysis”, 7th Edition, CBS Publications, 1986.
2. Skoog, D.A., Holler, F.J. and Nieman, T.A., “Principles of Instrumental Analysis”,
5th Edition, Harcourt College Publishers, 2001.
3. Settle, F., “Hand Book of Instrumental Techniques for Analytical Chemistry”,
Pearson Education (P) Ltd, 2004.
PY3311 INSTRUMENTAL METHODS OF PHARMACEUTICAL ANALYSIS
UNIT I UV – VISIBLE SPECTROSCOPY 9
Properties of electromagnetic spectrum – Chromophore concept – Beer’s and
Lambart’s law – Limitations – Theory of electronic spectroscopy – Choice of solvent and
solvent effects – Modern instrumentation – Design and working principle – Applications
of UV-Visible spectroscopy – Nephlometry and turbidimetry – Principle – Instrumentation
– Applications.
UNIT II INFRARED AND NMR SPECTROSCOPY 9
Principles of vibrational spectroscopy – Instrumentation and sampling techniques –
Applications in pharmaceutical sciences – NMR principles – Instrumentation –
Applications.
L T P C
0 0 3 2
L T P C
3 1 0 4
48
UNIT III MASS AND ATOMIC SPECTROSCOPY 9
Principles – Instrumentation – Ionization techniques – Electron impact ionization –
Chemical ionization – Applications – Atomic absorption spectroscopy – Principle –
Instrumentation – Applications.
UNIT IV CHROMATOGRAPHIC TECHNIQUES 9
Chromatographic methods – Paper chromatography – Thin layer chromatography – Ion
exchange chromatography – Column chromatography – High performance liquid
chromatography – Applications.
UNIT V ELCTROCHEMICAL METHODS OF ANALYSIS 9
Potentiometry – Types of electrodes – Measurement of EMF and pH – Applications –
Conductometry – Measurement of conductivity – Conductometric titrations.
L: 45 T: 15 TOTAL: 60 PERIODS
TEXT BOOKS
1. Beckett, A.K. and Stenlake, J.B., “Practical Pharmaceutical Chemistry”, Part I
and II, 4th Edition, CBS Publications, 1997.
2. Chatwal, G.R. and Anand, S.K., “Instrumental Methods of Chemical Analysis”,
Himalaya Publishing House, 2005.
REFERENCES
1. Willard, H.H., Merritt Jr, L.L., Dean, J.A. and Settle Jr, F.A., “Instrumental
Methods of Analysis”, 7th Edition, CBS Publications, 1986.
2. Skoog, D.A., Holler, F.J. and Nieman, T.A., “Principles of Instrumental Analysis”,
5th Edition, Harcourt College Publishers, 2001.
3. Settle, F., “Hand Book of Instrumental Techniques for Analytical Chemistry”,
Pearson Education (P) Ltd, 2004.
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