PM3302 INSTRUMENTATION AND INSTRUMENTAL ANALYSIS SYLLABUS | ANNA UNIVERSITY BE PETROCHEMICAL ENGINEERING 6TH SEMESTER SYLLABUS REGULATION 2008 2011 2012-2013 BELOW IS THE ANNA UNIVERSITY SIXTH SEMESTER B.E PETROCHEMICAL ENGINEERING DEPARTMENT SYLLABUS, TEXTBOOKS, REFERENCE BOOKS,EXAM PORTIONS,QUESTION BANK,PREVIOUS YEAR QUESTION PAPERS,MODEL QUESTION PAPERS, CLASS NOTES, IMPORTANT 2 MARKS, 8 MARKS, 16 MARKS TOPICS. IT IS APPLICABLE FOR ALL STUDENTS ADMITTED IN THE YEAR 2011 2012-2013 (ANNA UNIVERSITY CHENNAI,TRICHY,MADURAI, TIRUNELVELI,COIMBATORE), 2008 REGULATION OF ANNA UNIVERSITY CHENNAI AND STUDENTS ADMITTED IN ANNA UNIVERSITY CHENNAI DURING 2009
PM3302 INSTRUMENTATION AND INSTRUMENTAL ANALYSIS L T P C
4 0 0 4
UNIT I INTRODUCTION TO INSTRUMENTS, CHARACTERISTICS
AND SIGNAL CONDITIONING 12
Introduction to Instruments and Their representation: Introduction, Elements, Classification, Standards,
Calibration procedures Static and Dynamic Characteristics of Instruments, Specification of static
characteristics, Selection of instruments, Forcing functions, Formulation of First order and second order
system equations, Dynamic response Principals of Analog signal conditioning, converters, guidelines for
analog signal conditioning design , Principles of digital signal conditioning, computer interface, DACs,
ADCs, DAS hardware, DAS software, characteristics of digital data
UNIT II TEMPERATURE, PRESSURE, LEVEL MEASUREMENTS 12
Temperature measurement: Temperature scales, Non electrical methods, Electrical methods, Radiation
methods
Pressure measurement: Moderate pressure measurement, High pressure measurement, vacuum
measurement
Level measurement: measurement techniques for Liquids and slurries, advance measurement
techniques
UNIT III FLOW MEASUREMENTS AND STUDY OF VALVES 12
Flow measurement: Introduction, Review of Venturimeter, orifice meters, rotameters, Pitot tube, working
of turbine, vortex shedding, electromagnetic flow meters
53
Introduction to Advanced flow measurement techniques: Hot Wire anemometer, Laser Doppler
anemometer, Ultrasound, Particle image Velocimetry
Study of Valves: Types of Valves, Actuators, Positioners, Valve characteristics, Controllability and
Rangeability, Cavitation, Flashing, choking, Valve Sizing for incompressible fluids, compressible fluids,
Two phase flows
UNIT IV INTRODUCTION TO QUALITY CONTROL AND ANALYTICAL
TECHNIQUES 12
Need for Chemical analysis in Petroleum industry. Crude Assay. Standard Test Methods. Introduction to
principles of Analytical techniques: Spectroscopic Techniques, Chromatographic techniques,
Crystallography, electrochemical analysis, thermal analysis, electrophoresis, calorimetery, Hybrid
techniques
Miscellaneous measurements and analysis: density, viscosity, Refractormeter, pH and redox
potential measurements. Thermal conductivity gas analyzers. Oxygen determination. Orsat analysis
UNIT V WORKING AND INTERPRETATION OF INSTRUMENTAL
ANALYTICAL METHODS : I 12
Spectroscopic techniques: Atomic Absorption, X-ray, inductively coupled argon plasma (ICAP),
ultraviolet – visible (UV-VIS), fluorescence, infrared (IR), Raman spectroscopy, mass spectrometry
(MS),nuclear magnetic resonance (NMR)
Chromatographic Techniques: gas chromatography (GC), high pressure liquid chromatography, gel
permeation chromatograpghy (GPC) , thin layer chromatograpghy (TLC), super criticle fluid
chromatography (SFC)
Classification of spectroscopic and chromatographic techniques for Analysis of fuels
Working and Interpretation of Instrumental analytical methods: II
Lubricant Analysis: constituents of lubricants, characterization of lubricants by analytical
techniques, importance of elemental analysis in lubricants
TEXT BOOKS:
1. Eckman, D. P.; Industrial Instrumentation; Wiley Eastern, 1991.
2. Johnson, C.; Process Control Instrumentation Technology; 4th ed., Prentice-Hall
International.
3. Liptak, B. G., Venczel, K.; Instrument Engineer’s Handbook, Process Measurement; Chiltan
Book Company
REFERENCES
1. Nakra, B. C.; Chaudhary K. K.; Instrumentation Measurement and Analysis; Tata McGraw
Hill, New Delhi, 1998.
2. Patranabis, D.; Principles of Industrial Instrumentation; Tata McGraw Hill, New Delhi, 1996.
3. Silverstein, Bassler, Morrill; Spectrometric Identification of Organic Compounds; JohnWiley
Publication, 1991.
4. Gary J.H. and Handework G.E., “Petroleum Refining Technology and Economics”, Marcel
Dekker, Inc., 1984.
PM3302 INSTRUMENTATION AND INSTRUMENTAL ANALYSIS L T P C
4 0 0 4
UNIT I INTRODUCTION TO INSTRUMENTS, CHARACTERISTICS
AND SIGNAL CONDITIONING 12
Introduction to Instruments and Their representation: Introduction, Elements, Classification, Standards,
Calibration procedures Static and Dynamic Characteristics of Instruments, Specification of static
characteristics, Selection of instruments, Forcing functions, Formulation of First order and second order
system equations, Dynamic response Principals of Analog signal conditioning, converters, guidelines for
analog signal conditioning design , Principles of digital signal conditioning, computer interface, DACs,
ADCs, DAS hardware, DAS software, characteristics of digital data
UNIT II TEMPERATURE, PRESSURE, LEVEL MEASUREMENTS 12
Temperature measurement: Temperature scales, Non electrical methods, Electrical methods, Radiation
methods
Pressure measurement: Moderate pressure measurement, High pressure measurement, vacuum
measurement
Level measurement: measurement techniques for Liquids and slurries, advance measurement
techniques
UNIT III FLOW MEASUREMENTS AND STUDY OF VALVES 12
Flow measurement: Introduction, Review of Venturimeter, orifice meters, rotameters, Pitot tube, working
of turbine, vortex shedding, electromagnetic flow meters
53
Introduction to Advanced flow measurement techniques: Hot Wire anemometer, Laser Doppler
anemometer, Ultrasound, Particle image Velocimetry
Study of Valves: Types of Valves, Actuators, Positioners, Valve characteristics, Controllability and
Rangeability, Cavitation, Flashing, choking, Valve Sizing for incompressible fluids, compressible fluids,
Two phase flows
UNIT IV INTRODUCTION TO QUALITY CONTROL AND ANALYTICAL
TECHNIQUES 12
Need for Chemical analysis in Petroleum industry. Crude Assay. Standard Test Methods. Introduction to
principles of Analytical techniques: Spectroscopic Techniques, Chromatographic techniques,
Crystallography, electrochemical analysis, thermal analysis, electrophoresis, calorimetery, Hybrid
techniques
Miscellaneous measurements and analysis: density, viscosity, Refractormeter, pH and redox
potential measurements. Thermal conductivity gas analyzers. Oxygen determination. Orsat analysis
UNIT V WORKING AND INTERPRETATION OF INSTRUMENTAL
ANALYTICAL METHODS : I 12
Spectroscopic techniques: Atomic Absorption, X-ray, inductively coupled argon plasma (ICAP),
ultraviolet – visible (UV-VIS), fluorescence, infrared (IR), Raman spectroscopy, mass spectrometry
(MS),nuclear magnetic resonance (NMR)
Chromatographic Techniques: gas chromatography (GC), high pressure liquid chromatography, gel
permeation chromatograpghy (GPC) , thin layer chromatograpghy (TLC), super criticle fluid
chromatography (SFC)
Classification of spectroscopic and chromatographic techniques for Analysis of fuels
Working and Interpretation of Instrumental analytical methods: II
Lubricant Analysis: constituents of lubricants, characterization of lubricants by analytical
techniques, importance of elemental analysis in lubricants
TEXT BOOKS:
1. Eckman, D. P.; Industrial Instrumentation; Wiley Eastern, 1991.
2. Johnson, C.; Process Control Instrumentation Technology; 4th ed., Prentice-Hall
International.
3. Liptak, B. G., Venczel, K.; Instrument Engineer’s Handbook, Process Measurement; Chiltan
Book Company
REFERENCES
1. Nakra, B. C.; Chaudhary K. K.; Instrumentation Measurement and Analysis; Tata McGraw
Hill, New Delhi, 1998.
2. Patranabis, D.; Principles of Industrial Instrumentation; Tata McGraw Hill, New Delhi, 1996.
3. Silverstein, Bassler, Morrill; Spectrometric Identification of Organic Compounds; JohnWiley
Publication, 1991.
4. Gary J.H. and Handework G.E., “Petroleum Refining Technology and Economics”, Marcel
Dekker, Inc., 1984.
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