IB3212 INSTRUMENTAL METHODS OF ANALYSIS SYLLABUS | ANNA UNIVERSITY BTECH FOOD TECHNOLOGY 4TH SEM SYLLABUS REGULATION 2008 2011 2012-2013 BELOW IS THE ANNA UNIVERSITY FOURTH SEMESTER B TECH FOOD TECHNOLOGY DEPARTMENT SYLLABUS, TEXTBOOKS, REFERENCE BOOKS,EXAM PORTIONS,QUESTION BANK,PREVIOUS YEAR QUESTION PAPERS,MODEL QUESTION PAPERS, CLASS NOTES, IMPORTANT 2 MARKS, 8 MARKS, 16 MARKS TOPICS. IT IS APPLICABLE FOR ALL STUDENTS ADMITTED IN THE YEAR 2011 2012-2013 (ANNA UNIVERSITY CHENNAI,TRICHY,MADURAI, TIRUNELVELI,COIMBATORE), 2008 REGULATION OF ANNA UNIVERSITY CHENNAI AND STUDENTS ADMITTED IN ANNA UNIVERSITY CHENNAI DURING 2009
IB3212 INSTRUMENTAL METHODS OF ANALYSIS L T P C
3 0 0 3
AIM To introduce students to the principles and methods of biological instruments.
OBJECTIVE
To provide to the students the fundamentals of instrument knowledge and their
applications in biology.
UNIT I OPTICAL SPECTROSCOPY 10
Design of Experiments – Error Analysis – S/N ratio – Limit of Detection – UV –VIS
Spectroscopy, Applications, Instruments – single beam, double beam and Photo-diode array
– applications – IR & Raman – Uses – Design – FT-IR, Raman.
UNIT II CHROMATOGRAPHY 10
Distribution coefficients – solid-liquid, liquid-liquid and gas chromatography – theory of
chromatography-normal phase & reverse phase chromatography – gel permeation – ion
exchange & affinity chromatography – HPLC- Instrumentation & case studies.
UNIT III STRUCTURAL ELUCIDATION 10
Nuclear Magnetic Resonance – Introduction-spin states – 1H, 13C NMR – Instrumentationuse
in structural elucidation. Electron Paramagnetic Resonance-concept & instrumentation –
use in metal containing proteins & membrane studies. X-Ray : X-ray spectroscopy –Auger –
EELS Instrumentation & applications in Biology- X-ray diffraction- Instrumentation –small
molecule & macromalecular crystallography.
UNIT IV MASS SPECTROMETRY 10
Introduction – Instrumentation – CI, EI-Methods of Ionization- Methods for separation of Ions
– Method for Detection. MALDI - TOF, ESI and FT-MS.
UNIT V ELECTROCHEMICAL MEASUREMENTS 5
Different types of electrochemical apparatus – Measuring Electrode potentials- Red-Ox
proteins – Porous Silicon.
TOTAL : 45 PERIODS
TEXTBOOKS
1. Skoog, D.A., f.J. Holler and S.R. Crouch “Principles of Instrumental f Analysis”.6th
Edition, Thomson/Brooks/Cole, 2002.
2. Willard, H.H. etal., “Instrumental Methods of Analysis”.7th Edition. CBS Publishers, 1986.
3. Braun, Robert D. “Introduction to Instrumental Analysis” Pharma Book Syndicate, 1987.
4. Ewing, G.W. “Instrumental Methods of Chemical Analysis” 5th Edition, Tata McGraw-Hill,
1985
IB3212 INSTRUMENTAL METHODS OF ANALYSIS L T P C
3 0 0 3
AIM To introduce students to the principles and methods of biological instruments.
OBJECTIVE
To provide to the students the fundamentals of instrument knowledge and their
applications in biology.
UNIT I OPTICAL SPECTROSCOPY 10
Design of Experiments – Error Analysis – S/N ratio – Limit of Detection – UV –VIS
Spectroscopy, Applications, Instruments – single beam, double beam and Photo-diode array
– applications – IR & Raman – Uses – Design – FT-IR, Raman.
UNIT II CHROMATOGRAPHY 10
Distribution coefficients – solid-liquid, liquid-liquid and gas chromatography – theory of
chromatography-normal phase & reverse phase chromatography – gel permeation – ion
exchange & affinity chromatography – HPLC- Instrumentation & case studies.
UNIT III STRUCTURAL ELUCIDATION 10
Nuclear Magnetic Resonance – Introduction-spin states – 1H, 13C NMR – Instrumentationuse
in structural elucidation. Electron Paramagnetic Resonance-concept & instrumentation –
use in metal containing proteins & membrane studies. X-Ray : X-ray spectroscopy –Auger –
EELS Instrumentation & applications in Biology- X-ray diffraction- Instrumentation –small
molecule & macromalecular crystallography.
UNIT IV MASS SPECTROMETRY 10
Introduction – Instrumentation – CI, EI-Methods of Ionization- Methods for separation of Ions
– Method for Detection. MALDI - TOF, ESI and FT-MS.
UNIT V ELECTROCHEMICAL MEASUREMENTS 5
Different types of electrochemical apparatus – Measuring Electrode potentials- Red-Ox
proteins – Porous Silicon.
TOTAL : 45 PERIODS
TEXTBOOKS
1. Skoog, D.A., f.J. Holler and S.R. Crouch “Principles of Instrumental f Analysis”.6th
Edition, Thomson/Brooks/Cole, 2002.
2. Willard, H.H. etal., “Instrumental Methods of Analysis”.7th Edition. CBS Publishers, 1986.
3. Braun, Robert D. “Introduction to Instrumental Analysis” Pharma Book Syndicate, 1987.
4. Ewing, G.W. “Instrumental Methods of Chemical Analysis” 5th Edition, Tata McGraw-Hill,
1985
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