CH3216 PHYSICAL CHEMISTRY LAB SYLLABUS | ANNA UNIVERSITY BTECH PETROCHEMICAL TECHNOLOGY 4TH SEM SYLLABUS REGULATION 2008 2011 2012-2013 BELOW IS THE ANNA UNIVERSITY FOURTH SEMESTER B TECH PETROCHEMICAL TECHNOLOGY DEPARTMENT SYLLABUS, TEXTBOOKS, REFERENCE BOOKS,EXAM PORTIONS,QUESTION BANK,PREVIOUS YEAR QUESTION PAPERS,MODEL QUESTION PAPERS, CLASS NOTES, IMPORTANT 2 MARKS, 8 MARKS, 16 MARKS TOPICS. IT IS APPLICABLE FOR ALL STUDENTS ADMITTED IN THE YEAR 2011 2012-2013 (ANNA UNIVERSITY CHENNAI,TRICHY,MADURAI, TIRUNELVELI,COIMBATORE), 2008 REGULATION OF ANNA UNIVERSITY CHENNAI AND STUDENTS ADMITTED IN ANNA UNIVERSITY CHENNAI DURING 2009
CH3216 PHYSICAL CHEMISTRY LABORATORY
1. Molecular weight determination of Polymer by using
a) Rast’s Method
b) Viscometer
2. Partition Coefficient Studies
For Benzene – Water system
3. Phase rule Studies
Simple Eutectic system
4. Conductivity Studies
a) Precipitation Titration
b) Mixtures of acid – Strong Base Titration
5. EMF Studies
Estimation of Fe2+ by Potentiometric Titration
6. Kinetic Studies
a) Kinetic studies of Persulphate – Iodide reaction
b) Kinetic studies of Iodination of Acetone.
c) Determination of Rate constant of Acid catalyst hydrolysis of an Ester.
7. Polarimetry Studies - Kinetic study of Inversion of Cane sugar.
8. Adsorption Studies - Freundlich Adsorption Isotherm
9. Determination of Transition Temperature.
10. Determination of Critical solution temperature for the Phenol - Water system.
11. Determination of Saponification value of an oil.
12. To determine the moisture & volatile contents in a given coal sample by
proximate analysis.
13. pH metric measurements
a) To prepare buffer solutions and standardization of PHmeter (PH4 and 9)
b) Determine the molarity of HCI by pH-metrically, using 0.1 M Sodium
Hydroxide.
TOTAL: 45 PERIODS
CH3216 PHYSICAL CHEMISTRY LABORATORY
1. Molecular weight determination of Polymer by using
a) Rast’s Method
b) Viscometer
2. Partition Coefficient Studies
For Benzene – Water system
3. Phase rule Studies
Simple Eutectic system
4. Conductivity Studies
a) Precipitation Titration
b) Mixtures of acid – Strong Base Titration
5. EMF Studies
Estimation of Fe2+ by Potentiometric Titration
6. Kinetic Studies
a) Kinetic studies of Persulphate – Iodide reaction
b) Kinetic studies of Iodination of Acetone.
c) Determination of Rate constant of Acid catalyst hydrolysis of an Ester.
7. Polarimetry Studies - Kinetic study of Inversion of Cane sugar.
8. Adsorption Studies - Freundlich Adsorption Isotherm
9. Determination of Transition Temperature.
10. Determination of Critical solution temperature for the Phenol - Water system.
11. Determination of Saponification value of an oil.
12. To determine the moisture & volatile contents in a given coal sample by
proximate analysis.
13. pH metric measurements
a) To prepare buffer solutions and standardization of PHmeter (PH4 and 9)
b) Determine the molarity of HCI by pH-metrically, using 0.1 M Sodium
Hydroxide.
TOTAL: 45 PERIODS
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