CH 2258 PHYSICAL CHEMISTRY LAB SYLLABUS | ANNA UNIVERSITY BTECH CHEMICAL ENGINEERING 4TH SEM SYLLABUS REGULATION 2008 2011 2012-2013 BELOW IS THE ANNA UNIVERSITY FOURTH SEMESTER B.TECH CHEMICAL ENGINEERING DEPARTMENT SYLLABUS, TEXTBOOKS, REFERENCE BOOKS,EXAM PORTIONS,QUESTION BANK,PREVIOUS YEAR QUESTION PAPERS,MODEL QUESTION PAPERS, CLASS NOTES, IMPORTANT 2 MARKS, 8 MARKS, 16 MARKS TOPICS. IT IS APPLICABLE FOR ALL STUDENTS ADMITTED IN THE YEAR 2011 2012-2013 (ANNA UNIVERSITY CHENNAI,TRICHY,MADURAI, TIRUNELVELI,COIMBATORE), 2008 REGULATION OF ANNA UNIVERSITY CHENNAI AND STUDENTS ADMITTED IN ANNA UNIVERSITY CHENNAI DURING 2009
CH 2258 PHYSICAL CHEMISTRY LAB L T P C
0 0 3 2
AIM
To determine experimentally various properties of the chemical compounds and to
determine and estimate kinetics values, and other properties of chemicals.
OBJECTIVES : To improve the practical knowledge on the properties and
characteristics of solvents and mixtures.
LIST OF EXPERIMENTS
1. Determination of molecular weight of a polymer by viscosity method.
2. Determination of partition co-efficient of iodine between two immiscible solvents
3. Determination of partition co-efficient of benzoic acid between two immiscible
solvents
4. Determination of Ka of the weak acid
5. Conductometric experiments- Verification of Oswald’s Dilution Law
6. Titration of Strong Acid Vs Strong Base
7. Titration of mixture of Strong Acid Weak Acid Vs Strong Base
8. Titration of Weak Acid Vs Weak Base
9. Determination of Rate Constant (K)
10. Determination of Activation Energy (ΔE)
11. Estimation of Ferrous ion concentration by Potentiometric Titration
12. Determination of standard electrode potential (Zn, Cu, Ag)
13. Adsorption studies
14. To study the adsorption of Acetic acid on charcoal and construct the isotherm.
15. Determination of pH metric titration of Strong Acid Vs Strong Base
16. Enzyme catalytic reaction by varying pH.
17. Application of Phase Rule to Phenol-Water system
18. To study the inversion of cane sugar by polarimeter.
a. Polarimeter-Inversion of cane sugar
b. Refractometer
TOTAL: 45 PERIODS
38
REFERENCE BOOK :
1. Physical Chemistry experiments by Alexander Findley, McGraw-Hill IV Edition,
(1976).
LIST OF EQUIPMENTS
1. Micro Calorimeter
2. Beckman Thermometers. Glasswares,
3. Thermometers 0 to 110 – 0°. Bottle Shakers .pH meters
4. Pressure Glass bottles. Standard Cells. Multimeters
5. Viscometers-Ostwald Cannan Ubbelholde. Voltage Stabiliser
6. Stalalmometer
7. Surface Tension Meter .Tape Heaters
8. Mantle Heaters
9. DC Power Supply. Thermostat. Cyrostats
CH 2258 PHYSICAL CHEMISTRY LAB L T P C
0 0 3 2
AIM
To determine experimentally various properties of the chemical compounds and to
determine and estimate kinetics values, and other properties of chemicals.
OBJECTIVES : To improve the practical knowledge on the properties and
characteristics of solvents and mixtures.
LIST OF EXPERIMENTS
1. Determination of molecular weight of a polymer by viscosity method.
2. Determination of partition co-efficient of iodine between two immiscible solvents
3. Determination of partition co-efficient of benzoic acid between two immiscible
solvents
4. Determination of Ka of the weak acid
5. Conductometric experiments- Verification of Oswald’s Dilution Law
6. Titration of Strong Acid Vs Strong Base
7. Titration of mixture of Strong Acid Weak Acid Vs Strong Base
8. Titration of Weak Acid Vs Weak Base
9. Determination of Rate Constant (K)
10. Determination of Activation Energy (ΔE)
11. Estimation of Ferrous ion concentration by Potentiometric Titration
12. Determination of standard electrode potential (Zn, Cu, Ag)
13. Adsorption studies
14. To study the adsorption of Acetic acid on charcoal and construct the isotherm.
15. Determination of pH metric titration of Strong Acid Vs Strong Base
16. Enzyme catalytic reaction by varying pH.
17. Application of Phase Rule to Phenol-Water system
18. To study the inversion of cane sugar by polarimeter.
a. Polarimeter-Inversion of cane sugar
b. Refractometer
TOTAL: 45 PERIODS
38
REFERENCE BOOK :
1. Physical Chemistry experiments by Alexander Findley, McGraw-Hill IV Edition,
(1976).
LIST OF EQUIPMENTS
1. Micro Calorimeter
2. Beckman Thermometers. Glasswares,
3. Thermometers 0 to 110 – 0°. Bottle Shakers .pH meters
4. Pressure Glass bottles. Standard Cells. Multimeters
5. Viscometers-Ostwald Cannan Ubbelholde. Voltage Stabiliser
6. Stalalmometer
7. Surface Tension Meter .Tape Heaters
8. Mantle Heaters
9. DC Power Supply. Thermostat. Cyrostats
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