PT2302 ANALYSIS AND CHARACTERIZATION OF POLYMERS SYLLABUS | ANNA UNIVERSITY B.TECH. POLYMER TECHNOLOGY 5TH SEMESTER SYLLABUS REGULATION 2008 2011 2012-2013 BELOW IS THE ANNA UNIVERSITY FIFTH SEMESTER B.TECH. POLYMER TECHNOLOGY DEPARTMENT SYLLABUS, TEXTBOOKS, REFERENCE BOOKS, IT IS APPLICABLE FOR ALL STUDENTS ADMITTED IN THE YEAR 2011 2012-2013 (ANNA UNIVERSITY CHENNAI,TRICHY,MADURAI,TIRUNELVELI,COIMBATORE), 2008 REGULATION OF ANNA UNIVERSITY CHENNAI AND STUDENTS ADMITTED IN ANNA UNIVERSITY CHENNAI DURING 2009
PT2302 ANALYSIS AND CHARACTERISATION OF POLYMERS L T P C
3 0 0 3
AIM
To familiarize the techniques of identification and analysis of polymers
OBJECTIVES
To prepare the students with methodology for facing the industrial and academic
challenges in
Identifying various polymers
Controlling the quality of incoming raw materials and processing
Characterizing different fluid of polymers
Analyzing polymers through various instrumental methods
UNIT I IDENTIFICATION AND ANALYSIS 9
Identification of rubbers and plastics by simple physical methods by chemical analysis,
application of instrumental techniques for identification of polymers and additives
Thermoplastics – melting point, density, viscosity, melt flow index, K-value. Thermo sets
– moisture analysis, particle size, apparent density, spiral flow test, cup flow test, gel
time and peak exothermic temperature. Resins – acid value, hydroxyl value, isocyanate
index, epoxy equivalent
UNIT II SPECIFICATIONS, QUALITY CONTROL AND PROCESS ABILITY
TESTS 9
Rubber latex and dry rubber – cup viscosity, total alkalinity, total solids, dry rubber
content, volatile matter, KOH number, mechanical stability and heat stability, Plasticity,
plasticity retention index (PRI), scorch time and cure characteristics (plastimeter,
Mooney viscometer, oscillating disc rheometer)
UNIT III MOLECULAR CHARACTERIZATION OF POLYMERS 9
Determination of molecular weight, viscometry, end group analysis, colligative property,
osmometry light scattering technique, determination of molecular weight and molecular
weight distribution, gel permeation chromatography
UNIT IV THERMAL ANALYSIS OF POLYMERS 9
Differential thermal analysis (DTA), differential scanning calorimetry (DSC), thermo
gravimetric analysis (TGA), thermo mechanical analysis (TMA), dynamic mechanical
thermal analysis (DMTA)
UNIT V PHYSICAL METHODS OF ANALYSIS 9
X-ray diffraction (Wide angle and small angle), Infrared spectroscopy (IR & FTIR), and
Nuclear magnetic resonance spectrometer (NMR), GC – Mass spectrometer, optical
microscopy, scanning electron microscopy, and transmission electron microscopy
TOTAL: 45 PERIODS
TEXT BOOK
1. Chermisinoff, Polymer Characterization – Laboratory Techniques and Analysis.
Hunt & James, Polymer Characterization, Chapman & Hall, London, 1993
REFERENCES
1. Hoffman, Rubber technology Handbook, Hanser Publishers, Munich 1996
2. ASTM - 9.01 & 9.02; 8.01 & 8.04, 2000
3. Kampff, Characterization of Plastics using physical methods, Experimental
Techniques and practical applications
4. D. Campbell & J.R. White, Polymer Characterization, Chapman & Hall, 1989.
PT2302 ANALYSIS AND CHARACTERISATION OF POLYMERS L T P C
3 0 0 3
AIM
To familiarize the techniques of identification and analysis of polymers
OBJECTIVES
To prepare the students with methodology for facing the industrial and academic
challenges in
Identifying various polymers
Controlling the quality of incoming raw materials and processing
Characterizing different fluid of polymers
Analyzing polymers through various instrumental methods
UNIT I IDENTIFICATION AND ANALYSIS 9
Identification of rubbers and plastics by simple physical methods by chemical analysis,
application of instrumental techniques for identification of polymers and additives
Thermoplastics – melting point, density, viscosity, melt flow index, K-value. Thermo sets
– moisture analysis, particle size, apparent density, spiral flow test, cup flow test, gel
time and peak exothermic temperature. Resins – acid value, hydroxyl value, isocyanate
index, epoxy equivalent
UNIT II SPECIFICATIONS, QUALITY CONTROL AND PROCESS ABILITY
TESTS 9
Rubber latex and dry rubber – cup viscosity, total alkalinity, total solids, dry rubber
content, volatile matter, KOH number, mechanical stability and heat stability, Plasticity,
plasticity retention index (PRI), scorch time and cure characteristics (plastimeter,
Mooney viscometer, oscillating disc rheometer)
UNIT III MOLECULAR CHARACTERIZATION OF POLYMERS 9
Determination of molecular weight, viscometry, end group analysis, colligative property,
osmometry light scattering technique, determination of molecular weight and molecular
weight distribution, gel permeation chromatography
UNIT IV THERMAL ANALYSIS OF POLYMERS 9
Differential thermal analysis (DTA), differential scanning calorimetry (DSC), thermo
gravimetric analysis (TGA), thermo mechanical analysis (TMA), dynamic mechanical
thermal analysis (DMTA)
UNIT V PHYSICAL METHODS OF ANALYSIS 9
X-ray diffraction (Wide angle and small angle), Infrared spectroscopy (IR & FTIR), and
Nuclear magnetic resonance spectrometer (NMR), GC – Mass spectrometer, optical
microscopy, scanning electron microscopy, and transmission electron microscopy
TOTAL: 45 PERIODS
TEXT BOOK
1. Chermisinoff, Polymer Characterization – Laboratory Techniques and Analysis.
Hunt & James, Polymer Characterization, Chapman & Hall, London, 1993
REFERENCES
1. Hoffman, Rubber technology Handbook, Hanser Publishers, Munich 1996
2. ASTM - 9.01 & 9.02; 8.01 & 8.04, 2000
3. Kampff, Characterization of Plastics using physical methods, Experimental
Techniques and practical applications
4. D. Campbell & J.R. White, Polymer Characterization, Chapman & Hall, 1989.
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