CH2307 TECHNICAL ANALYSIS LAB SYLLABUS | ANNA UNIVERSITY B.TECH. CHEMICAL ENGINEERING 5TH SEMESTER SYLLABUS REGULATION 2008 2011 2012-2013

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CH2307 TECHNICAL ANALYSIS LAB SYLLABUS | ANNA UNIVERSITY B.TECH. CHEMICAL ENGINEERING 5TH SEMESTER SYLLABUS REGULATION 2008 2011 2012-2013 BELOW IS THE ANNA UNIVERSITY FIFTH SEMESTER B.TECH. CHEMICAL ENGINEERING DEPARTMENT SYLLABUS, TEXTBOOKS, REFERENCE BOOKS, IT IS APPLICABLE FOR ALL STUDENTS ADMITTED IN THE YEAR 2011 2012-2013 (ANNA UNIVERSITY CHENNAI,TRICHY,MADURAI,TIRUNELVELI,COIMBATORE), 2008 REGULATION OF ANNA UNIVERSITY CHENNAI AND STUDENTS ADMITTED IN ANNA UNIVERSITY CHENNAI DURING 2009


CH2307 TECHNICAL ANALYSIS LAB L T P C
0 0 3 2
AIM
To determine experimentally the various elements and compounds used in chemical
engineering
OBJECTIVES
 To have a thorough understanding on the estimation and analysis of chemical
compounds.
LIST OF EXPERIMENTS
1. Ore Analysis
 Estimation of manganese in pyrolusite ore.
 Estimation of magnesium in dolomite.
2. Analysis of alloys .
3. Analysis of fertilizer.
 Estimation of nitrogen in urea by kjeldal method.
4. Sugar Analysis .
5. Estimation of phenol by Iodimetry / UV-Vis Spectrometer.
6. Water Analysis
 Determination of total residual chlorine in water.
 Determination of chemical oxygen demand.
 Determination of dissolved oxygen.
7. Polymer analysis .
8. Conductometric Titration.
9. Potentiometry.
 Estimation of iron.
 Determination of standard – electrode potential of Zn , Fe , Copper.
10. Estimation of sodium and potassium by flame photometry.
11. Gravimetric analysis
 Estimation of barium in barium sulphate.
 Estimation of nickel as DMG.
12. pH metry (acid – basic titration ) – not basic.
* Minimum 10 experiments shall be offered TOTAL : 45 PERIODS
INSTRUMENTS REQUIRED
1. UV/Vis Spectrophotometer
2. Colorimeter
3. pH meter
4. Flame photometer
5. Conductivity meter
6. Glass electrodes
7. Kjeldal’s apparatus
8. Potentiometer